I-2-chloro-1 - (1-chlorocyclopropyl) i-ethyl ketone
Ulwazi olusisiseko:
Igama lekhemikhali: 2-chloro-1 -(1-chlorocyclopropyl) ethyl ketone; I-Chloroacetyl chlorocyclopropane;
Inombolo ye-CAS: 120983-72-4
Ifomula yemolekyuli: C5H6Cl2O
Ubunzima bemolekyuli: 153.01
Inombolo ye-EINECS: 446-620-9
Ifomula yolwakhiwo:
Iindidi eziyeleleneyo: Abaphakathi - abaphakathi kwezibulali zinambuzane; Imichiza ekrwada; Iziphakathi zeekhemikhali; Organic ichiza ekrwada;
Indawo yokubila: 202.0±20.0 °C(Kuqikelelwe)
Ubuninzi: 1.35± 0.1g /cm3(Kuqikelelwe)
Uxinzelelo lomphunga: 80Pa kwi25℃
Ukunyibilika kwamanzi: 5.91g/L ku-20℃
Iipropati: Ulwelo olungenambala okanye olukhanyayo olutyheli. Kulula ukugqwala, ivumba elicaphukisayo.
LogP: 1.56570
| Sukucaciswa | Unit | Sumgangatho |
| Imbonakalo | Ulwelo olungenambala ukuya kolutyheli | |
| Umxholo ophambili | % | ≥95.0%;90%; |
| Ukufuma | % | ≤0.5 |
I-2-chloro-1 -(1-chlorocyclopropyl) i-ethyl ketone yikhemikhali ebalulekileyo ephakathi, enye yezona zinto zibalulekileyo kwi-synthesis yeprothiobacillazole. Iprothiobacillazole luhlobo olutsha lwesibulali-sikhundi esibanzi setriazolthione, esisetyenziswa ikakhulu ukulawula izifo zeesiriyeli, ingqolowa kunye neembotyi. Inobutyhefu obulungileyo bebhayoloji kunye nendalo, ubuthi obuphantsi, akukho teratogenic okanye uhlobo lwe-mutagenic, akukho tyhefu kwiimbumba, kunye nokhuseleko kumzimba womntu kunye nokusingqongileyo.
I-118.5g ye-1-(1-chlorocyclopropyl) ethyl ketone, i-237mL ye-dichloromethane kunye ne-9.6g ye-methanol zithathwe kwi-reactor ye-500mL, kwaye ubushushu behliswa ukuya kwi-0℃. Irhasi yeklorini yafakwa kwisixokelelwano kwaye ubushushu bokusabela bugcinwe bungaphantsi kwe-5℃. Emva kwe-3h yegesi ye-chlorine, igesi ye-chlorine iye yamiswa kwaye ukugcinwa kobushushu kwaqhubeka i-30min. Emva kokusabela, irhasi ye-chlorine eshiyekileyo kunye ne-hydrogen chloride kwinkqubo yatsalwa kwi-0 ℃ phantsi koxinzelelo olubi lwe-1h, kwaye i-solvent yasuswa nge-vacuum distillation kwi-25 ℃ / -0.1Mpa ukufumana ulwelo oluphuzi olukhanyayo 2-chloro. -1 -(1-chlorocyclopropyl) ethyl ketone enesivuno se-92.5% kunye nomxholo we-93.8%.
25Kg okanye 200Kg / umgqomo; Ukupakisha ngokweemfuno zomthengi.
Le mveliso kufuneka igcinwe ipholile, ifakwe umoya, yomile, kwaye ikhuselwe ngokungqongqo kumswakama, ukuvezwa kunye nemvula ngexesha lokugcinwa kunye nokuthutha, kwaye akufanele ixutywe kunye ne-oxidants yokuthutha kunye nokugcinwa.
